******************************************************************************
       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 R100193_powder_pattern
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  0.710710
 Wavelength #2 =  0.709270
 Wavelength #3 =  0.713590
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.184
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    7.5491 5.258792   0  2  0    2    7.5289  5.272559   -0.0202 -0.013768
   10.7846 3.710473   0  2  1    2   10.7788  3.712421   -0.0058 -0.001948
   14.2329 2.826153   1  1  0    2   14.2363  2.825495    0.0034  0.000658
   15.4068 2.614535   0  0  2    2   15.4099  2.614019    0.0031  0.000517
   16.2397 2.482788   1  1  1    2   16.2203  2.485700   -0.0194 -0.002912
   17.9329 2.252427   1  3  0    2   17.9374  2.251874    0.0045  0.000554
   19.5391 2.070599   1  3  1    2   19.5624  2.068178    0.0233  0.002420
   23.0942 1.757794   0  6  0    2   23.0979  1.757520    0.0037  0.000274
   25.0028 1.626509   1  5  1    2   24.9919  1.627201   -0.0109 -0.000692

 rmse = 0.00031985126
 
     A =2.933(2)               B =10.545(5)               C =5.228(5)            
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 161.7(2)