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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070589
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.001
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   28.0950 3.173588   1  1  2    2   28.0886  3.174292   -0.0064 -0.000704
   41.4135 2.178549   0  6  1    2   41.4077  2.178842   -0.0058 -0.000293
   19.8783 4.463019   1  2  0    2   19.8730  4.464207   -0.0053 -0.001188
   33.8152 2.648660   1  3  2    2   33.8100  2.649053   -0.0052 -0.000393
   38.8353 2.317040   2  1  2    2   38.8311  2.317279   -0.0042 -0.000240
   36.5319 2.457677   0  2  3    2   36.5279  2.457935   -0.0040 -0.000257
   27.3053 3.263556   1  3  1    2   27.3022  3.263917   -0.0031 -0.000361
   35.0927 2.555107   2  2  1    2   35.0899  2.555307   -0.0028 -0.000200
   53.2564 1.718649  -3  2  2    2   53.2539  1.718725   -0.0025 -0.000076
   24.7213 3.598531   1  3  0    2   24.7196  3.598770   -0.0017 -0.000239
   36.2240 2.477859   2  3  0    2   36.2228  2.477941   -0.0012 -0.000082
   22.4680 3.954089   0  0  2    2   22.4668  3.954289   -0.0012 -0.000200
   51.6311 1.768866  -3  3  1    2   51.6304  1.768888   -0.0007 -0.000022
   27.6996 3.217987  -1  1  2    2   27.7007  3.217861    0.0011  0.000126
   57.4476 1.602820  -2  5  3    2   57.4487  1.602791    0.0011  0.000029
   18.8518 4.703672   1  0  1    2   18.8531  4.703343    0.0013  0.000330
   56.2566 1.633896   1  8  0    2   56.2580  1.633857    0.0014  0.000039
   30.8991 2.891665   2  1  0    2   30.9007  2.891519    0.0016  0.000147
   52.1972 1.751005   2  6  1    2   52.1989  1.750951    0.0017  0.000054
   32.7859 2.729427  -2  1  1    2   32.7892  2.729162    0.0033  0.000265
   37.0824 2.422446  -1  0  3    2   37.0862  2.422207    0.0038  0.000239
   26.1867 3.400377   0  4  0    2   26.1909  3.399836    0.0042  0.000541
   23.4053 3.797811   0  1  2    2   23.4102  3.797031    0.0049  0.000780
   16.3164 5.428472   1  1  0    2   16.3217  5.426736    0.0053  0.001736
   22.9678 3.869158   1  2  1    2   22.9739  3.868149    0.0061  0.001009
   17.1761 5.158634   0  2  1    2   17.1851  5.155960    0.0090  0.002673
   40.5485 2.223005   2  2  2    2   40.5580  2.222505    0.0095  0.000501

 rmse = 0.00003528178
 
     A =5.9191(2)              B =13.5993(5)              C =7.9095(5)           
 Alpha =90                  Beta =90.895(4)           Gamma =90                  
 
 Volume = 636.61(4)