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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050309
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.068
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   24.8743 3.586240   1  1  2    2   24.8673  3.587242   -0.0070 -0.001002
   25.3585 3.518666   0  2  2    2   25.3485  3.520031   -0.0100 -0.001365
   28.9653 3.087161   2  2  1    2   28.9743  3.086225    0.0090  0.000936
   31.0597 2.883139   2  0  2    2   31.0658  2.882583    0.0061  0.000556
   32.2250 2.781270   1  3  2    2   32.2327  2.780622    0.0077  0.000648
   34.7003 2.587937   0  2  3    2   34.7018  2.587831    0.0015  0.000106
   35.7469 2.514385   0  4  2    2   35.7433  2.514633   -0.0036 -0.000249
   36.8198 2.443407   3  1  1    2   36.8140  2.443777   -0.0058 -0.000371

 rmse = 0.00006221525
 
     A =7.817(1)               B =12.448(4)               C =8.536(2)            
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 830.7(0)