Stottite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from single crystal data of R120089 Ross C R, Bernstein L R, Waychunas G A American Mineralogist 73 (1988) 657-661 Crystal-structure refinement of stottite, FeGe(OH)6 _database_code_amcsd 0001167 CELL PARAMETERS: 7.5510 7.5510 7.4650 90.000 90.000 90.000 ALTERNATE SETTING FOR SPACE GROUP: P4_2/n ATOM X Y Z OCCUPANCY ISO(B) Fe 0.00000 0.00000 0.00000 1.000 0.647 Ge 0.50000 0.00000 0.00000 1.000 0.564 OH 0.26700 0.44300 0.58300 1.000 1.231 OH 0.57300 0.26800 0.56500 1.000 1.002 OH 0.43700 0.42100 0.26700 1.000 1.200 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 6 +/- 6 +/- 6 MAX. ABS. INTENSITY / VOLUME**2: 47.33138677 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 20.45 8.13 4.3428 1 1 1 23.56 100.00 3.7755 2 0 0 23.84 45.84 3.7325 0 0 2 33.57 19.31 2.6697 2 2 0 33.77 41.91 2.6543 2 0 2 37.72 4.87 2.3851 3 0 1 38.08 4.58 2.3633 1 0 3 39.63 4.88 2.2743 3 1 1 39.63 1.54 2.2743 1 3 1 41.59 19.01 2.1714 2 2 2 44.95 1.81 2.0164 3 2 1 45.27 1.58 2.0032 1 2 3 48.21 14.25 1.8878 4 0 0 48.80 6.13 1.8663 0 0 4 54.33 10.62 1.6885 4 2 0 54.33 7.75 1.6885 2 4 0 54.47 19.11 1.6846 4 0 2 54.88 18.27 1.6730 2 0 4 60.15 11.13 1.5384 2 4 2 60.15 14.75 1.5384 4 2 2 60.53 13.42 1.5296 2 2 4 70.55 2.92 1.3348 4 4 0 71.02 5.02 1.3272 4 0 4 74.34 1.06 1.2759 3 5 1 75.67 4.63 1.2569 4 4 2 76.01 4.62 1.2521 2 4 4 76.01 3.96 1.2521 4 2 4 80.44 1.44 1.1939 6 2 0 80.44 2.11 1.1939 2 6 0 80.55 3.81 1.1925 6 0 2 81.45 3.52 1.1817 2 0 6 85.36 4.03 1.1372 2 6 2 85.36 4.09 1.1372 6 2 2 86.25 4.21 1.1277 2 2 6 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.