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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 Experimental R060978
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  0.710710
 Wavelength #2 =  0.709270
 Wavelength #3 =  0.713590
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.042
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   31.6003 1.304155   3  1  1    2   31.6146  1.303581    0.0143  0.000574
   27.2763 1.506329  -1  1  3    2   27.2875  1.505724    0.0112  0.000605
   20.8755 1.961438  -1  1  2    2   20.8836  1.960682    0.0081  0.000756
   14.8502 2.752023   1  1  0    2   14.8551  2.751112    0.0049  0.000911
   37.9450 1.091975  -1  3  1    2   37.9455  1.091961    0.0005  0.000015
   34.5587 1.195354  -2  0  4    2   34.5561  1.195441   -0.0026 -0.000087
   36.9180 1.121286  -4  0  2    2   36.9140  1.121404   -0.0040 -0.000119
   23.9496 1.712222   0  2  0    2   23.9375  1.713078   -0.0121 -0.000856
   25.9669 1.581009   2  0  2    2   25.9485  1.582110   -0.0184 -0.001102

 rmse = 0.00042598661
 
     A =4.679(1)               B =3.4262(9)               C =5.134(2)            
 Alpha =90                  Beta =99.39(3)            Gamma =90                  
 
 Volume = 81.19(4)