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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 2461b-processed X-ray powder diffraction
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.015
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   13.5367 6.528730   1  1  0    2   13.5412  6.526579    0.0045  0.002151
   14.3836 6.146563  -1  0  1    2   14.3859  6.145600    0.0023  0.000963
   15.3952 5.745268   0 -1  1    2   15.3961  5.744916    0.0009  0.000351
   19.2696 4.598843   0  2  0    2   19.2634  4.600317   -0.0062 -0.001474
   20.0504 4.421615  -1  1  1    2   20.0474  4.422275   -0.0030 -0.000661
   22.5020 3.945430   1  1  1    2   22.4985  3.946028   -0.0035 -0.000598
   29.0186 3.072989  -2  0  2    2   29.0204  3.072800    0.0018  0.000189
   29.5176 3.022192  -2  1  1    2   29.5190  3.022053    0.0014  0.000139
   29.9575 2.978829  -2 -3  1    2   29.9632  2.978273    0.0057  0.000556
   33.5988 2.663995   2  0  1    2   33.6016  2.663782    0.0028  0.000213
   34.4893 2.597252  -3 -2  1    2   34.4847  2.597586   -0.0046 -0.000334
   37.5294 2.393632   0 -3  2    2   37.5276  2.393745   -0.0018 -0.000114
   38.9121 2.311732   1 -3  1    2   38.9127  2.311697    0.0006  0.000036
   48.4605 1.876346  -2  2  3    2   48.4604  1.876348   -0.0001 -0.000002

 rmse = 0.00002776396
 
     A =7.9501(7)              B =9.974(1)                C =7.634(1)            
 Alpha =103.86(1)           Beta =115.835(9)          Gamma =67.855(7)           
 
 Volume = 502.57(6)