Tinticite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern of R190028 Rius J, Louer D, Louer M, Gali S, Melgarejo J C European Journal of Mineralogy 12 (2000) 581-588 Structure solution from powder data of the phosphate hydrate tinticite _database_code_amcsd 0006835 CELL PARAMETERS: 7.950119 9.974243 7.633709 103.8645 115.8350 67.85474 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 505.086 Density (g/cm3): 2.915 MAX. ABS. INTENSITY / VOLUME**2: 6.684669975 RIR: 0.747 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.91 40.71 6.8426 0 0 1 13.00 6.20 6.7986 1 0 0 13.54 23.38 6.5266 1 1 0 14.10 1.20 6.2688 -1 -1 1 14.39 41.00 6.1456 -1 0 1 15.40 60.44 5.7449 0 -1 1 19.26 38.93 4.6003 0 2 0 19.43 4.92 4.5623 -1 -2 1 19.61 2.55 4.5201 1 2 0 20.05 5.16 4.4223 -1 1 1 21.65 5.13 4.0993 1 0 1 22.26 13.63 3.9883 0 -2 1 22.44 10.51 3.9570 -2 -1 1 22.50 81.10 3.9460 1 1 1 23.53 2.42 3.7761 -1 -1 2 24.23 1.35 3.6673 0 2 1 24.59 1.03 3.6158 -2 -2 1 24.90 1.41 3.5712 2 1 0 26.18 3.25 3.3993 2 0 0 26.53 4.30 3.3552 -1 2 0 26.69 28.03 3.3360 -1 -2 2 26.93 100.00 3.3059 0 -1 2 27.01 2.33 3.2963 -2 -1 2 27.09 6.24 3.2869 1 2 1 27.29 7.15 3.2633 2 2 0 27.90 20.50 3.1938 1 3 0 28.10 18.59 3.1715 -1 2 1 28.44 2.30 3.1344 -2 -2 2 28.61 9.34 3.1161 0 1 2 29.02 33.15 3.0728 -2 0 2 29.08 1.28 3.0669 0 3 0 29.52 80.09 3.0221 -2 1 1 29.96 47.96 2.9783 -2 -3 1 30.71 1.01 2.9075 -2 1 0 31.06 1.25 2.8753 1 -2 1 31.09 2.17 2.8725 0 -2 2 32.64 2.27 2.7399 -1 -3 2 32.62 4.18 2.7418 2 3 0 33.03 3.79 2.7087 0 3 1 33.60 4.38 2.6638 2 0 1 34.04 7.66 2.6304 1 3 1 34.42 1.09 2.6022 1 1 2 34.48 9.43 2.5976 -3 -2 1 35.02 6.49 2.5589 -1 2 2 35.18 8.69 2.5479 2 2 1 35.63 2.34 2.5168 -1 3 0 35.59 8.34 2.5195 -1 -1 3 36.35 4.28 2.4685 -1 -4 1 36.37 6.27 2.4670 -1 0 3 36.63 3.13 2.4505 -3 0 1 37.00 1.72 2.4267 2 -1 1 37.31 1.12 2.4069 -2 -4 1 37.43 1.14 2.3995 -2 2 0 37.53 19.66 2.3937 0 -3 2 37.52 1.16 2.3940 -3 -3 1 38.01 11.05 2.3643 1 2 2 38.10 13.89 2.3592 -2 0 3 38.18 5.04 2.3545 -3 -3 2 38.25 2.78 2.3502 -3 0 2 38.37 3.72 2.3432 3 2 0 38.91 4.05 2.3117 1 -3 1 39.46 2.21 2.2812 -2 -4 2 39.73 3.70 2.2662 3 0 0 39.73 1.02 2.2663 -1 1 3 39.80 1.77 2.2621 0 -1 3 39.84 3.44 2.2599 1 -2 2 39.87 2.89 2.2586 2 3 1 40.17 1.05 2.2423 0 -4 1 40.32 2.64 2.2343 -2 -3 3 40.76 3.92 2.2111 -2 2 2 41.22 8.14 2.1875 0 3 2 42.58 19.63 2.1208 2 -2 1 42.57 9.51 2.1212 0 -2 3 42.79 4.68 2.1111 -3 -4 1 43.09 3.29 2.0969 -3 -4 2 43.20 26.14 2.0919 -3 1 2 43.25 2.50 2.0896 -3 -3 3 43.71 2.36 2.0684 1 3 2 44.13 3.76 2.0497 2 0 2 45.25 10.16 2.0015 -2 3 1 45.55 3.51 1.9893 -2 3 0 45.71 18.25 1.9825 -2 -4 3 45.81 3.05 1.9785 -4 -2 2 45.87 6.94 1.9760 -2 -5 1 45.95 2.24 1.9730 2 2 2 46.15 2.77 1.9646 1 -3 2 46.39 2.66 1.9550 2 4 1 46.56 9.80 1.9485 1 0 3 46.62 15.83 1.9460 3 4 0 47.07 1.09 1.9285 -4 -3 2 47.43 2.39 1.9146 -2 -5 2 47.42 4.81 1.9150 0 -3 3 47.77 7.65 1.9017 -2 -1 4 48.46 15.46 1.8763 -2 2 3 49.07 1.19 1.8544 -1 -5 2 49.07 5.45 1.8544 3 3 1 49.72 6.53 1.8316 -3 -5 2 49.71 2.69 1.8321 -3 -5 1 49.76 1.83 1.8304 2 -3 1 50.04 1.54 1.8208 -1 -2 4 50.29 1.66 1.8123 3 -1 1 50.42 1.86 1.8079 -4 -4 2 51.07 2.10 1.7864 1 -2 3 51.48 7.96 1.7731 4 1 0 51.59 1.51 1.7696 1 5 1 52.03 1.00 1.7558 0 3 3 52.16 1.28 1.7517 -1 4 2 52.60 2.28 1.7380 0 5 1 52.56 1.37 1.7393 -1 1 4 53.21 4.96 1.7194 -3 0 4 53.30 2.36 1.7169 -1 -3 4 53.31 1.56 1.7165 -2 1 4 53.51 9.26 1.7107 0 0 4 53.88 1.03 1.6997 4 0 0 53.93 1.14 1.6982 0 -4 3 54.38 2.83 1.6854 0 -5 2 54.71 1.03 1.6759 -4 1 1 55.18 7.97 1.6629 -3 -4 4 55.26 1.07 1.6607 -3 2 3 55.59 1.09 1.6514 -1 -5 3 55.60 2.94 1.6511 -1 5 0 55.54 1.58 1.6529 0 -2 4 55.51 1.60 1.6537 1 3 3 55.61 4.08 1.6510 3 1 2 55.96 2.36 1.6413 -3 3 1 56.53 1.51 1.6262 3 2 2 56.55 1.35 1.6258 2 1 3 57.01 3.15 1.6136 -4 -1 4 57.84 7.76 1.5924 -3 3 2 57.90 1.06 1.5910 -3 -6 1 58.07 1.10 1.5867 -5 -2 2 58.11 1.95 1.5858 -2 4 2 58.15 4.56 1.5847 2 -4 1 58.12 1.92 1.5854 -4 1 0 58.34 1.74 1.5801 -4 1 3 59.05 1.16 1.5627 0 5 2 59.24 3.88 1.5580 0 2 4 59.33 7.73 1.5560 3 3 2 59.54 9.68 1.5511 -5 -2 3 59.50 4.17 1.5519 3 -1 2 59.67 1.10 1.5479 -5 -1 2 60.29 5.76 1.5334 0 6 0 60.49 5.74 1.5289 -5 -3 1 60.62 1.81 1.5261 0 -6 1 60.94 8.20 1.5187 -2 -6 3 60.88 2.43 1.5200 -2 -1 5 60.99 1.62 1.5175 -4 2 1 61.28 2.85 1.5110 -4 2 2 61.34 3.50 1.5097 -5 -1 1 61.48 1.96 1.5067 -5 -4 3 61.48 6.77 1.5067 3 6 0 61.61 3.22 1.5038 1 6 1 61.60 1.18 1.5041 4 5 0 61.98 1.97 1.4957 1 4 3 62.28 1.01 1.4891 -4 -6 2 62.22 2.24 1.4904 2 3 3 62.81 1.73 1.4779 1 -4 3 62.88 4.69 1.4764 -2 -3 5 63.06 1.17 1.4726 -5 0 2 63.14 1.47 1.4711 -4 -5 4 63.16 1.75 1.4707 2 5 2 63.26 3.58 1.4684 2 6 1 63.96 1.42 1.4540 -1 0 5 64.25 1.31 1.4481 -5 -2 4 64.71 3.71 1.4390 -2 4 3 64.81 1.54 1.4370 -2 5 1 64.85 1.37 1.4362 0 -4 4 64.90 1.02 1.4354 -5 0 3 65.01 2.36 1.4332 -4 1 4 65.12 1.26 1.4309 5 2 0 66.10 3.01 1.4122 -2 1 5 66.24 3.89 1.4094 -3 4 0 66.75 2.56 1.3999 -3 -7 2 66.83 2.65 1.3985 -5 -5 1 67.11 2.77 1.3933 -3 -6 4 67.33 1.32 1.3892 2 -3 3 68.41 2.33 1.3700 -2 -6 4 68.93 2.20 1.3608 1 6 2 68.95 1.08 1.3605 3 2 3 68.95 1.25 1.3605 1 3 4 69.24 1.03 1.3556 -5 1 1 69.93 2.34 1.3439 3 5 2 70.37 1.57 1.3366 -5 -6 3 71.51 8.69 1.3181 -5 -3 5 71.51 1.70 1.3180 -6 -3 2 72.44 1.45 1.3034 1 7 1 73.11 3.78 1.2931 5 2 1 74.42 1.27 1.2736 2 5 3 74.95 2.77 1.2659 0 -7 2 76.02 1.08 1.2507 -6 -4 1 75.94 1.35 1.2518 1 0 5 76.40 1.13 1.2453 5 0 1 76.48 1.66 1.2443 5 4 1 76.88 3.35 1.2387 -4 -2 6 77.27 1.22 1.2335 -2 0 6 77.78 2.07 1.2267 -2 3 5 78.84 1.17 1.2129 -1 -8 1 78.80 1.07 1.2133 4 -2 2 78.89 1.39 1.2122 1 6 3 79.58 1.20 1.2035 -4 -8 2 80.54 2.16 1.1914 0 7 2 80.63 1.20 1.1904 6 3 0 82.29 1.72 1.1705 2 -5 3 82.39 1.25 1.1694 1 -3 5 82.62 1.26 1.1667 3 0 4 84.08 1.22 1.1501 0 8 0 84.19 1.54 1.1489 1 3 5 84.59 2.07 1.1445 0 -1 6 86.68 1.11 1.1222 -2 -7 5 88.68 1.19 1.1020 0 -3 6 89.52 1.87 1.0938 0 6 4 89.87 1.04 1.0905 -4 5 0 89.87 1.04 1.0905 -4 5 0 XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.