Tintinaite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from single crystal data of R110046 Miehe G Nature Physical Science 231 (1971) 133-134 Crystal structure of kobellite Locality: Korunka mine, Spissko-Gemerske Rudohorie Mountains, Czechoslovakia _database_code_amcsd 0014683 CELL PARAMETERS: 34.0360 22.5040 4.0339 90.000 90.182 90.000 SPACE GROUP: Pnnm ATOM X Y Z OCCUPANCY ISO(B) Cu 0.13070 0.33540 0.50000 0.444 3.500 Fe 0.13070 0.33540 0.50000 0.556 3.500 Pb 0.27360 0.03520 0.50000 1.000 2.700 Pb 0.15560 0.13220 0.50000 1.000 3.100 Pb 0.06390 0.24660 0.50000 1.000 2.800 Pb 0.26750 0.37200 0.00000 1.000 3.800 Pb 0.45820 0.36210 0.00000 1.000 2.800 Pb 0.11390 0.43820 0.00000 1.000 3.500 Bi 0.05270 0.04510 0.00000 0.333 2.400 Sb 0.05270 0.04510 0.00000 0.667 2.400 Bi 0.43810 0.04400 0.00000 0.833 2.400 Sb 0.43810 0.04400 0.00000 0.167 2.400 Bi 0.32680 0.14040 0.00000 0.556 2.000 Sb 0.32680 0.14040 0.00000 0.444 2.000 Bi 0.48730 0.15020 0.50000 0.667 2.500 Sb 0.48730 0.15020 0.50000 0.333 2.500 Bi 0.23390 0.24120 0.00000 0.556 1.900 Sb 0.23390 0.24120 0.00000 0.444 1.900 Bi 0.39500 0.25510 0.50000 0.500 2.000 Sb 0.39500 0.25510 0.50000 0.500 2.000 Bi 0.36690 0.45470 0.50000 0.500 2.600 Sb 0.36690 0.45470 0.50000 0.500 2.600 S 0.50000 0.00000 0.50000 1.000 1.800 S 0.13280 0.04590 0.50000 1.000 2.100 S 0.37810 0.08540 0.50000 1.000 1.100 S 0.23700 0.09530 0.00000 1.000 1.200 S 0.05400 0.11800 0.00000 1.000 1.200 S 0.13890 0.20240 0.00000 1.000 1.000 S 0.28380 0.18220 0.50000 1.000 1.500 S 0.44930 0.19970 0.00000 1.000 1.500 S 0.48900 0.29410 0.50000 1.000 1.100 S 0.35380 0.29650 0.00000 1.000 1.400 S 0.20770 0.28730 0.50000 1.000 1.700 S 0.08740 0.31580 0.00000 1.000 1.300 S 0.03330 0.40090 0.50000 1.000 2.300 S 0.18710 0.39140 0.50000 1.000 1.100 S 0.36690 0.38140 0.50000 1.000 1.700 S 0.28460 0.44990 0.00000 1.000 1.300 S 0.45750 0.44820 0.00000 1.000 1.000 S 0.15320 0.49540 0.50000 1.000 2.100 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 31 +/- 20 +/- 3 MAX. ABS. INTENSITY / VOLUME**2: 38.39319828 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 5.19 5.91 17.0179 2 0 0 11.07 1.42 7.9891 3 2 0 12.08 1.87 7.3255 1 3 0 12.90 2.10 6.8641 2 3 0 13.04 5.63 6.7869 4 2 0 14.15 2.59 6.2573 3 3 0 15.21 5.58 5.8243 5 2 0 15.62 14.20 5.6726 6 0 0 16.11 4.84 5.5006 6 1 0 18.67 3.60 4.7526 7 1 0 18.91 2.88 4.6930 4 4 0 19.62 72.84 4.5246 6 3 0 19.89 32.35 4.4634 7 2 0 20.48 42.30 4.3366 5 4 0 20.88 4.26 4.2545 8 0 0 21.78 10.71 4.0801 7 3 0 22.25 68.04 3.9946 6 4 0 22.35 7.37 3.9785 4 5 0 22.39 5.96 3.9706 0 1 1 22.54 1.31 3.9453 -1 1 1 22.55 1.31 3.9424 1 1 1 22.98 7.94 3.8694 -2 1 1 23.02 7.91 3.8641 2 1 1 23.57 3.31 3.7751 -1 2 1 23.58 3.30 3.7726 1 2 1 23.70 3.97 3.7544 5 5 0 23.72 14.48 3.7514 -3 1 1 23.72 2.59 3.7507 0 6 0 23.76 14.41 3.7441 3 1 1 23.86 11.78 3.7295 9 1 0 24.00 5.65 3.7085 -2 2 1 24.03 5.63 3.7037 2 2 1 24.05 2.24 3.7007 8 3 0 24.70 1.88 3.6041 -3 2 1 24.71 9.87 3.6024 -4 1 1 24.75 1.87 3.5977 3 2 1 24.77 9.80 3.5938 4 1 1 24.84 2.73 3.5847 9 2 0 25.01 3.98 3.5611 3 6 0 25.06 11.34 3.5528 0 3 1 25.26 31.55 3.5258 6 5 0 25.60 16.60 3.4797 -2 3 1 25.63 16.55 3.4758 2 3 1 25.63 2.94 3.4752 -5 0 1 25.66 4.81 3.4715 -4 2 1 25.71 2.91 3.4655 5 0 1 25.72 4.78 3.4638 4 2 1 25.94 12.32 3.4344 -5 1 1 25.96 4.03 3.4320 4 6 0 26.01 12.23 3.4251 5 1 1 26.18 23.62 3.4036 10 0 0 26.26 33.05 3.3931 -3 3 1 26.31 32.91 3.3877 3 3 1 26.49 7.01 3.3653 10 1 0 27.00 5.33 3.3029 7 5 0 27.15 100.00 3.2850 5 6 0 27.17 1.49 3.2817 -4 3 1 27.23 1.48 3.2752 4 3 1 27.32 3.23 3.2640 -1 4 1 27.34 3.23 3.2624 1 4 1 27.38 2.65 3.2578 10 2 0 27.70 6.20 3.2206 -2 4 1 27.73 6.18 3.2176 2 4 1 28.24 41.59 3.1599 -6 2 1 28.25 1.57 3.1590 2 7 0 28.30 24.70 3.1532 -5 3 1 28.32 24.03 3.1516 -3 4 1 28.32 41.26 3.1512 6 2 1 28.36 23.94 3.1473 3 4 1 28.37 24.53 3.1460 5 3 1 28.44 1.52 3.1386 9 4 0 28.53 31.06 3.1286 6 6 0 28.71 2.46 3.1094 -7 0 1 28.80 2.44 3.0997 7 0 1 28.80 1.43 3.0995 10 3 0 28.88 1.31 3.0918 8 5 0 29.13 18.45 3.0653 11 1 0 29.74 5.52 3.0039 0 5 1 29.85 1.97 2.9929 -1 5 1 29.87 1.97 2.9917 1 5 1 29.95 15.15 2.9834 11 2 0 30.23 4.18 2.9566 -5 4 1 30.29 4.15 2.9506 5 4 1 30.70 1.28 2.9121 10 4 0 30.75 16.98 2.9073 -8 1 1 30.76 3.73 2.9070 5 7 0 30.85 16.82 2.8983 8 1 1 31.27 14.42 2.8604 11 3 0 31.48 10.87 2.8416 -6 4 1 31.53 1.58 2.8372 -8 2 1 31.54 3.01 2.8363 12 0 0 31.56 10.79 2.8352 6 4 1 31.63 1.57 2.8288 8 2 1 31.80 11.64 2.8141 12 1 0 31.81 6.11 2.8130 0 8 0 31.92 1.92 2.8034 1 8 0 32.00 18.05 2.7969 6 7 0 32.25 2.32 2.7753 2 8 0 32.40 47.99 2.7633 -9 0 1 32.50 47.54 2.7546 9 0 1 32.56 7.98 2.7503 12 2 0 33.04 5.95 2.7112 11 4 0 33.39 1.33 2.6836 -9 2 1 33.41 3.97 2.6817 7 7 0 33.49 1.31 2.6756 9 2 1 33.55 12.62 2.6710 -3 6 1 33.55 5.10 2.6708 4 8 0 33.59 12.58 2.6683 3 6 1 33.79 27.01 2.6530 12 3 0 34.28 19.30 2.6156 -4 6 1 34.33 19.22 2.6123 4 6 1 34.59 7.69 2.5930 -9 3 1 34.66 3.84 2.5881 -10 1 1 34.69 7.62 2.5857 9 3 1 34.77 3.81 2.5801 10 1 1 35.19 1.23 2.5500 13 2 0 35.20 4.33 2.5498 11 5 0 35.21 2.94 2.5491 -5 6 1 35.26 2.93 2.5453 5 6 1 35.36 17.28 2.5383 -10 2 1 35.44 1.12 2.5327 12 4 0 35.47 17.12 2.5307 10 2 1 35.71 9.55 2.5141 0 7 1 35.81 1.03 2.5076 -1 7 1 35.82 1.03 2.5069 1 7 1 36.02 3.57 2.4937 1 9 0 36.10 1.79 2.4878 -2 7 1 36.13 1.78 2.4864 2 7 1 36.22 2.21 2.4803 -9 4 1 36.31 2.19 2.4740 9 4 1 36.31 2.92 2.4739 2 9 0 36.34 4.27 2.4719 13 3 0 36.51 6.55 2.4612 -10 3 1 36.58 1.14 2.4567 -8 5 1 36.59 34.33 2.4556 -3 7 1 36.61 6.50 2.4543 10 3 1 36.63 34.24 2.4535 3 7 1 36.66 1.13 2.4512 8 5 1 36.77 2.21 2.4443 -11 1 1 36.88 2.19 2.4369 11 1 1 36.92 3.73 2.4349 7 8 0 37.27 12.05 2.4124 -4 7 1 37.32 12.01 2.4098 4 7 1 37.44 4.50 2.4022 -11 2 1 37.55 4.46 2.3952 11 2 1 37.57 1.08 2.3938 -7 6 1 37.65 1.08 2.3893 7 6 1 37.69 2.61 2.3868 11 6 0 37.90 2.83 2.3737 13 4 0 38.06 2.68 2.3642 -10 4 1 38.16 2.65 2.3581 10 4 1 39.13 5.16 2.3024 -1 8 1 39.14 5.16 2.3018 1 8 1 39.83 3.17 2.2631 13 5 0 39.85 2.87 2.2619 -3 8 1 39.88 2.86 2.2603 3 8 1 39.94 1.03 2.2571 9 8 0 40.02 4.01 2.2531 -11 4 1 40.07 27.20 2.2504 0 10 0 40.12 3.97 2.2473 11 4 1 40.16 1.63 2.2455 1 10 0 40.35 3.59 2.2350 -7 7 1 40.42 3.43 2.2317 14 4 0 40.42 3.57 2.2314 7 7 1 40.43 1.81 2.2310 2 10 0 40.46 4.21 2.2294 11 7 0 40.49 2.03 2.2280 -4 8 1 40.53 2.02 2.2259 4 8 1 40.55 1.33 2.2247 -9 6 1 40.56 2.43 2.2243 15 2 0 40.64 1.32 2.2201 9 6 1 41.58 4.21 2.1719 15 3 0 41.65 2.23 2.1683 10 8 0 42.09 6.74 2.1468 13 6 0 42.23 2.09 2.1398 -10 6 1 42.26 3.36 2.1387 -6 8 1 42.31 3.35 2.1360 6 8 1 42.33 2.07 2.1353 10 6 1 42.50 12.51 2.1269 12 7 0 43.17 5.64 2.0956 -9 7 1 43.25 2.29 2.0918 6 10 0 43.25 5.60 2.0918 9 7 1 43.30 2.69 2.0896 -3 9 1 43.33 2.68 2.0883 3 9 1 43.38 2.84 2.0858 9 9 0 44.36 2.92 2.0421 1 11 0 44.64 1.10 2.0301 13 7 0 44.65 4.35 2.0297 -5 9 1 44.69 4.33 2.0277 5 9 1 44.77 2.45 2.0241 -10 7 1 44.86 2.43 2.0203 10 7 1 44.94 66.97 2.0169 0 0 2 44.99 3.93 2.0151 10 9 0 45.13 1.05 2.0090 -14 3 1 45.26 1.04 2.0037 14 3 1 45.41 5.47 1.9973 12 8 0 45.48 2.63 1.9942 17 1 0 45.59 1.62 1.9898 16 4 0 46.01 3.26 1.9727 -15 1 1 46.04 2.16 1.9713 -9 8 1 46.12 2.15 1.9681 9 8 1 46.14 3.23 1.9674 15 1 1 46.44 1.77 1.9552 -14 4 1 46.57 1.33 1.9504 -15 2 1 46.57 1.76 1.9504 14 4 1 46.61 2.26 1.9486 -7 9 1 46.67 2.25 1.9462 7 9 1 46.70 1.31 1.9452 15 2 1 46.79 1.60 1.9414 15 6 0 47.26 3.34 1.9232 16 5 0 47.48 6.76 1.9147 -15 3 1 47.57 2.32 1.9115 -10 8 1 47.61 6.69 1.9099 15 3 1 47.66 2.30 1.9083 10 8 1 47.81 1.67 1.9025 -8 9 1 47.88 1.66 1.9000 8 9 1 47.95 1.20 1.8972 -13 6 1 48.06 1.19 1.8931 13 6 1 48.12 6.17 1.8909 18 0 0 48.49 5.26 1.8775 -16 1 1 48.50 1.81 1.8772 10 10 0 48.54 2.54 1.8756 12 9 0 48.55 3.40 1.8753 0 12 0 48.62 5.21 1.8727 16 1 1 48.75 16.09 1.8680 -15 4 1 48.87 15.94 1.8635 15 4 1 49.03 2.83 1.8579 -6 10 1 49.08 2.82 1.8561 6 10 1 49.15 1.05 1.8538 15 7 0 49.22 1.08 1.8513 -11 8 1 49.24 1.25 1.8504 16 6 0 49.31 1.07 1.8481 11 8 1 49.43 4.96 1.8439 -6 3 2 49.43 1.72 1.8437 8 11 0 49.53 4.92 1.8405 6 3 2 49.54 2.18 1.8400 -7 2 2 49.66 2.16 1.8360 7 2 2 49.73 6.75 1.8335 18 3 0 49.82 3.20 1.8302 -5 4 2 49.90 3.18 1.8274 5 4 2 50.05 2.30 1.8224 -14 6 1 50.12 1.25 1.8200 11 10 0 50.16 2.28 1.8185 14 6 1 50.47 1.52 1.8083 13 9 0 50.60 3.44 1.8040 -10 9 1 50.66 6.12 1.8021 -6 4 2 50.66 2.32 1.8018 -3 11 1 50.68 3.42 1.8013 10 9 1 50.69 2.32 1.8010 3 11 1 50.75 6.08 1.7988 6 4 2 51.02 1.39 1.7900 -17 1 1 51.13 1.48 1.7866 -16 4 1 51.16 1.38 1.7855 17 1 1 51.17 2.45 1.7852 -8 10 1 51.19 1.53 1.7846 -4 11 1 51.22 1.52 1.7835 4 11 1 51.23 2.43 1.7831 8 10 1 51.26 1.46 1.7824 16 4 1 51.44 1.06 1.7764 -9 1 2 51.58 1.05 1.7718 9 1 2 51.67 2.88 1.7691 19 2 0 52.20 3.34 1.7522 -6 5 2 52.24 4.05 1.7512 -15 6 1 52.28 1.93 1.7497 7 12 0 52.30 3.32 1.7492 6 5 2 52.35 4.02 1.7475 15 6 1 52.39 1.40 1.7463 -17 3 1 52.44 8.46 1.7450 -9 10 1 52.49 2.43 1.7433 18 5 0 52.51 8.42 1.7427 9 10 1 52.53 1.38 1.7421 17 3 1 52.68 2.50 1.7376 -10 0 2 52.84 2.48 1.7327 10 0 2 53.26 11.60 1.7200 -5 6 2 53.34 11.54 1.7176 5 6 2 53.71 5.13 1.7065 11 11 0 53.83 2.49 1.7031 -10 10 1 53.91 2.47 1.7008 10 10 1 54.05 4.00 1.6966 -6 6 2 54.15 3.97 1.6939 6 6 2 54.20 3.21 1.6923 2 12 1 54.37 2.33 1.6874 -11 1 2 54.42 1.67 1.6861 -15 7 1 54.53 1.66 1.6828 15 7 1 54.54 2.30 1.6825 11 1 2 54.71 1.02 1.6778 -8 11 1 54.77 1.02 1.6760 8 11 1 54.87 2.01 1.6733 -11 2 2 55.04 1.99 1.6686 11 2 2 55.36 1.03 1.6596 20 3 0 55.37 3.82 1.6592 12 11 0 55.50 4.86 1.6557 6 13 0 55.68 2.15 1.6506 -11 3 2 55.85 2.12 1.6461 11 3 2 55.98 3.75 1.6425 10 12 0 56.01 1.91 1.6418 -12 1 2 56.11 1.90 1.6391 0 8 2 56.18 2.68 1.6372 -6 7 2 56.19 1.89 1.6369 12 1 2 56.28 2.67 1.6347 6 7 2 56.42 4.95 1.6308 7 13 0 56.46 1.86 1.6299 18 7 0 56.47 1.45 1.6295 -6 12 1 56.50 1.26 1.6288 -12 2 2 56.52 1.44 1.6283 6 12 1 56.68 1.24 1.6241 12 2 2 56.82 1.17 1.6202 16 9 0 56.96 2.76 1.6166 21 1 0 57.30 4.44 1.6079 -12 3 2 57.44 2.46 1.6042 21 2 0 57.46 1.45 1.6038 11 12 0 57.48 4.38 1.6033 12 3 2 58.04 2.54 1.5891 1 13 1 58.24 11.44 1.5841 2 13 1 58.59 2.39 1.5756 -3 13 1 58.61 2.39 1.5751 3 13 1 58.88 1.25 1.5684 1 9 2 59.11 1.63 1.5628 17 9 0 59.27 1.31 1.5591 -18 6 1 59.40 1.30 1.5559 18 6 1 59.45 1.44 1.5547 -20 2 1 59.55 1.88 1.5524 -15 9 1 59.60 1.42 1.5512 20 2 1 59.66 1.86 1.5498 15 9 1 59.67 1.55 1.5495 -5 13 1 59.71 1.54 1.5486 5 13 1 59.80 5.15 1.5465 6 14 0 60.23 1.27 1.5365 -20 3 1 60.38 1.25 1.5331 20 3 1 60.68 1.10 1.5262 7 14 0 61.36 1.79 1.5110 19 8 0 61.75 2.56 1.5022 -21 1 1 61.76 11.36 1.5020 0 10 2 61.90 2.54 1.4989 21 1 1 62.42 1.29 1.4877 2 14 1 62.75 3.61 1.4807 3 14 1 62.90 1.16 1.4776 12 13 0 62.97 2.23 1.4761 -21 3 1 63.12 2.21 1.4730 21 3 1 63.17 1.55 1.4719 -13 6 2 63.35 1.53 1.4681 13 6 2 63.49 2.96 1.4653 -12 7 2 63.66 2.93 1.4618 12 7 2 64.02 1.20 1.4544 -21 4 1 64.15 1.65 1.4518 23 3 0 64.17 1.19 1.4514 21 4 1 64.35 2.89 1.4477 18 10 0 64.50 1.21 1.4446 -16 10 1 64.62 1.20 1.4424 16 10 1 64.98 1.35 1.4352 1 11 2 65.36 2.89 1.4278 -21 5 1 65.50 2.87 1.4250 21 5 1 65.72 1.32 1.4208 -12 8 2 65.89 1.31 1.4176 12 8 2 66.01 1.27 1.4154 24 1 0 66.49 1.94 1.4062 0 15 1 67.45 1.11 1.3886 18 11 0 67.59 1.61 1.3859 -16 11 1 67.70 1.60 1.3839 16 11 1 67.83 1.65 1.3817 -18 0 2 68.07 4.11 1.3774 5 16 0 68.07 1.10 1.3774 -5 15 1 68.08 1.62 1.3773 18 0 2 68.10 1.10 1.3768 5 15 1 68.12 1.18 1.3765 23 6 0 68.20 1.62 1.3751 24 4 0 68.29 1.78 1.3734 0 12 2 68.86 3.68 1.3635 -21 7 1 68.97 1.68 1.3617 -15 12 1 69.00 3.65 1.3610 21 7 1 69.07 1.67 1.3599 15 12 1 69.13 1.88 1.3588 -18 3 2 69.37 1.85 1.3546 18 3 2 71.78 1.20 1.3151 -3 3 3 71.84 1.19 1.3141 3 3 3 71.95 1.65 1.3124 4 16 1 72.49 1.54 1.3039 -11 11 2 72.53 1.65 1.3033 -15 13 1 72.63 1.64 1.3018 15 13 1 72.64 1.53 1.3017 11 11 2 72.71 1.45 1.3005 -6 2 3 72.83 1.44 1.2987 6 2 3 73.90 1.23 1.2825 -12 11 2 74.05 1.54 1.2803 -6 13 2 74.05 1.22 1.2802 12 11 2 74.12 1.53 1.2792 6 13 2 74.28 1.17 1.2768 18 13 0 74.42 1.59 1.2747 -16 13 1 74.44 1.21 1.2746 -10 12 2 74.53 1.59 1.2732 16 13 1 74.57 1.20 1.2727 10 12 2 74.83 1.65 1.2688 -7 13 2 74.87 2.51 1.2682 -9 0 3 74.92 1.64 1.2675 7 13 2 75.05 2.48 1.2657 9 0 3 75.98 1.12 1.2525 -4 6 3 76.05 1.11 1.2514 4 6 3 76.14 1.54 1.2502 3 17 1 76.30 2.17 1.2480 -15 14 1 76.39 2.16 1.2467 15 14 1 76.56 2.29 1.2444 -26 1 1 76.57 1.00 1.2443 -10 2 3 76.73 2.27 1.2421 26 1 1 77.36 2.23 1.2335 -3 7 3 77.42 2.22 1.2328 3 7 3 77.79 1.87 1.2278 -6 14 2 77.87 1.87 1.2268 6 14 2 81.80 1.13 1.1774 -18 10 2 82.03 1.12 1.1747 18 10 2 85.30 1.69 1.1378 -5 16 2 85.37 1.69 1.1371 5 16 2 85.60 1.81 1.1346 -15 4 3 85.89 1.78 1.1316 15 4 3 88.29 1.01 1.1068 7 19 1 88.50 1.09 1.1048 -9 10 3 88.67 1.08 1.1032 9 10 3 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.