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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060004
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.062
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    8.9358 9.957395   0  0  2    2    8.9303  9.963522   -0.0055 -0.006127
   17.8810 4.973702   0  0  4    2   17.8519  4.981761   -0.0291 -0.008059
   20.5813 4.324849  -2  0  2    2   20.5888  4.323276    0.0075  0.001573
   24.6353 3.619753  -2  0  4    2   24.6292  3.620641   -0.0061 -0.000889
   25.6652 3.476431  -1  1  4    2   25.6700  3.475791    0.0048  0.000640
   26.8876 3.320723   0  0  6    2   26.8839  3.321174   -0.0037 -0.000451
   27.9378 3.197955   1  1  4    2   27.9191  3.200062   -0.0187 -0.002107
   29.1015 3.072394   2  0  4    2   29.1161  3.070887    0.0146  0.001507
   31.2845 2.862375   1  1  5    2   31.3009  2.860913    0.0164  0.001462
   40.9799 2.203744   2  2  1    2   40.9806  2.203709    0.0007  0.000035
   44.0128 2.058445  -3  1  7    2   44.0122  2.058473   -0.0006 -0.000028
   45.5391 1.992844   0  0 10    2   45.5425  1.992704    0.0034  0.000140
   54.9101 1.672454   3  1  8    2   54.9062  1.672562   -0.0039 -0.000108

 rmse = 0.00008699149
 
     A =8.990(3)               B =5.185(2)                C =20.202(3)           
 Alpha =90                  Beta =99.46(1)            Gamma =90                  
 
 Volume = 928.8(0)