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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050226
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.047
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   24.4819 3.639852   2  1  1    2   24.4864  3.639196    0.0045  0.000656
   26.1382 3.412426   1  1  2    2   26.1370  3.412582   -0.0012 -0.000156
   27.5179 3.244094   2  0  2    2   27.5166  3.244250   -0.0013 -0.000156
   29.5111 3.029016  -1  2  1    2   29.5091  3.029216   -0.0020 -0.000200
   34.6132 2.592709  -2  2  2    2   34.6149  2.592586    0.0017  0.000123
   35.7898 2.510013  -3  2  1    2   35.7884  2.510108   -0.0014 -0.000095
   43.0411 2.101980   0  3  1    2   43.0414  2.101964    0.0003  0.000015
   45.1372 2.009015   2  0  4    2   45.1372  2.009013    0.0000  0.000002

 rmse = 0.00001904334
 
     A =    12.036(2)          B =     6.4646(3)          C =     9.965(1)       
 Alpha =    90.             Beta =   106.75(1)        Gamma =    90.             
 
 Volume =    742.5(1)