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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050615
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.025
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   24.3675 3.653447   2  1  1    2   24.3564  3.655086   -0.0111 -0.001639
   27.4214 3.252738   2  0  2    2   27.4109  3.253959   -0.0105 -0.001221
   29.2818 3.049997  -1  2  1    2   29.2829  3.049881    0.0011  0.000116
   31.1001 2.875553  -4  0  2    2   31.0987  2.875683   -0.0014 -0.000129
   31.5425 2.836192   2  2  0    2   31.5341  2.836931   -0.0084 -0.000739
   34.3548 2.610015  -2  2  2    2   34.3565  2.609887    0.0017  0.000127
   35.5260 2.526547  -3  2  1    2   35.5300  2.526268    0.0040  0.000278
   36.1566 2.483885  -2  0  4    2   36.1609  2.483600    0.0043  0.000285
   40.4460 2.229645  -5  1  2    2   40.4479  2.229545    0.0019  0.000100
   42.7104 2.116460   0  3  1    2   42.7166  2.116166    0.0062  0.000294
   44.9595 2.015611   2  0  4    2   44.9649  2.015382    0.0054  0.000228
   63.1776 1.471025  -2  3  5    2   63.1736  1.471109   -0.0040 -0.000085

 rmse = 0.00005788012
 
     A =12.102(2)              B =6.5093(6)               C =10.015(1)           
 Alpha =90                  Beta =106.94(1)           Gamma =90                  
 
 Volume = 754.7(1)