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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060935
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.018
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   24.1601 3.683287  -3  1  1    2   24.1693  3.681900    0.0092  0.001387
   25.7376 3.460843  -3  1  2    2   25.7338  3.461348   -0.0038 -0.000506
   27.0406 3.296853  -4  0  2    2   27.0429  3.296573    0.0023  0.000280
   29.2651 3.050965   0  2  1    2   29.2641  3.051071   -0.0010 -0.000106
   30.8769 2.895186  -3  1  3    2   30.8727  2.895568   -0.0042 -0.000381
   31.1118 2.873848   2  0  2    2   31.1111  2.873912   -0.0007 -0.000064
   31.4921 2.839986   2  2  0    2   31.4890  2.840262   -0.0031 -0.000276
   32.6013 2.745797   3  1  1    2   32.6067  2.745354    0.0054  0.000443
   33.1350 2.702756  -2  2  2    2   33.1349  2.702764   -0.0001 -0.000008
   34.3174 2.612243   0  2  2    2   34.3214  2.611944    0.0040  0.000299
   35.5299 2.525782   2  2  1    2   35.5182  2.526586   -0.0117 -0.000804
   35.8924 2.501087  -2  0  4    2   35.8940  2.500981    0.0016  0.000106
   41.5983 2.170110  -4  2  3    2   41.6016  2.169947    0.0033  0.000163
   42.6726 2.117907  -1  3  1    2   42.6751  2.117789    0.0025  0.000119
   44.3105 2.043316  -6  0  4    2   44.3086  2.043399   -0.0019 -0.000083

 rmse = 0.00004336894
 
     A =13.422(2)              B =6.5105(5)               C =10.105(1)           
 Alpha =90                  Beta =119.975(7)          Gamma =90                  
 
 Volume = 764.9(1)