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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050425
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.041
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   13.2815 6.681163   1  1  0    2   13.2758  6.684014   -0.0057 -0.002851
   17.6811 5.023522   0  1  1    2   17.6776  5.024522   -0.0035 -0.001000
   21.1407 4.207022   2  1  1    2   21.1410  4.206956    0.0003  0.000066
   24.4663 3.641237  -4  1  1    2   24.4667  3.641175    0.0004  0.000062
   25.4416 3.503595  -2  0  2    2   25.4509  3.502329    0.0093  0.001266
   26.6909 3.342122   2  2  0    2   26.6918  3.342007    0.0009  0.000115
   27.0572 3.297634   5  1  0    2   27.0605  3.297240    0.0033  0.000394
   29.6788 3.011642  -3  1  2    2   29.6735  3.012168   -0.0053 -0.000526
   32.0521 2.793570  -6  1  1    2   32.0512  2.793650   -0.0009 -0.000080
   35.1352 2.554890  -6  0  2    2   35.1299  2.555267   -0.0053 -0.000377
   46.4241 1.955974  -3  2  3    2   46.4224  1.956041   -0.0017 -0.000066
   51.4935 1.774535 -10  0  2    2   51.4949  1.774489    0.0014  0.000047
   57.2522 1.608839   8  2  2    2   57.2544  1.608783    0.0022  0.000056
   57.5776 1.600512  -2  2  4    2   57.5795  1.600463    0.0019  0.000049
   70.8314 1.329869   9  2  3    2   70.8297  1.329897   -0.0017 -0.000028
   87.3072 1.116284   0  2  6    2   87.3071  1.116286   -0.0001 -0.000001

 rmse = 0.00002977747
 
     A =    18.8546(7)         B =     7.1641(9)          C =     7.1568(2)      
 Alpha =    90.             Beta =    99.972(3)       Gamma =    90.             
 
 Volume =    952.12(9)