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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R040185
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.012
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   11.1853 7.912707   1  1  0    2   11.1871  7.911412    0.0018  0.001295
   13.2333 6.691222   0  2  0    2   13.2202  6.697813   -0.0131 -0.006591
   18.0915 4.902626   2  0  0    2   18.0940  4.901943    0.0025  0.000682
   21.8744 4.062095   1  3  0    2   21.8663  4.063586   -0.0081 -0.001491
   23.1285 3.844476  -2  0  1    2   23.1293  3.844348    0.0008  0.000128
   27.9553 3.190386  -1  3  1    2   27.9635  3.189474    0.0082  0.000912
   30.0978 2.967886  -3  1  1    2   30.1022  2.967459    0.0044  0.000426
   36.9491 2.431592  -4  0  1    2   36.9482  2.431646   -0.0009 -0.000054
   39.2893 2.291933  -1  1  2    2   39.2860  2.292120   -0.0033 -0.000187
   55.9622 1.642094   1  5  2    2   55.9632  1.642068    0.0010  0.000026
   57.5508 1.600476  -5  5  1    2   57.5500  1.600496   -0.0008 -0.000019

 rmse = 0.00003695725
 
     A =10.147(1)              B =13.396(2)               C =4.6549(4)           
 Alpha =90                  Beta =104.94(2)           Gamma =90                  
 
 Volume = 611.32(6)