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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R040176
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.032
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   10.2078 8.685812   0  2  0    2   10.2197  8.675659    0.0119  0.010153
   10.5339 8.416821   1  1  0    2   10.5418  8.410544    0.0079  0.006277
   15.6836 5.657158   1  0  1    2   15.6913  5.654385    0.0077  0.002773
   16.4984 5.379014   1  1  1    2   16.5073  5.376126    0.0089  0.002888
   17.9082 4.957846   1  3  0    2   17.9139  4.956276    0.0057  0.001571
   18.4661 4.809037   2  0  0    2   18.4707  4.807844    0.0046  0.001192
   20.4851 4.338645   0  4  0    2   20.4890  4.337830    0.0039  0.000816
   21.9945 4.043757   1  3  1    2   21.9974  4.043223    0.0029  0.000533
   22.4558 3.961600   2  0  1    2   22.4568  3.961421    0.0010  0.000179
   23.0465 3.861238   2  1  1    2   23.0416  3.862047   -0.0049 -0.000809
   27.2946 3.268448   2  3  1    2   27.2958  3.268309    0.0012  0.000139
   27.7057 3.220821   2  4  0    2   27.7068  3.220694    0.0011  0.000127
   28.3288 3.151297   3  1  0    2   28.3232  3.151904   -0.0056 -0.000606
   29.0725 3.072265   1  2  2    2   29.0730  3.072211    0.0005  0.000054
   30.2284 2.957240   1  5  1    2   30.2240  2.957662   -0.0044 -0.000422
   30.5699 2.924943   2  4  1    2   30.5673  2.925185   -0.0026 -0.000242
   30.9318 2.891506   0  6  0    2   30.9276  2.891886   -0.0042 -0.000381
   31.9261 2.803594   3  3  0    2   31.9270  2.803515    0.0009  0.000080
   34.8536 2.574301   1  6  1    2   34.8482  2.574691   -0.0054 -0.000390
   35.3381 2.540077   2  3  2    2   35.3395  2.539980    0.0014  0.000097
   37.4087 2.403979   4  0  0    2   37.4096  2.403922    0.0009  0.000057
   38.0894 2.362532   3  0  2    2   38.0921  2.362372    0.0027  0.000160
   39.6467 2.273171   4  0  1    2   39.6449  2.273273   -0.0018 -0.000102
   46.2935 1.960853   3  7  0    2   46.2944  1.960816    0.0009  0.000037
   49.8305 1.829547   3  6  2    2   49.8311  1.829527    0.0006  0.000020
   52.3411 1.747490   0  0  4    2   52.3344  1.747697   -0.0067 -0.000207
   57.8709 1.592877   2  9  2    2   57.8729  1.592827    0.0020  0.000050
   58.7688 1.570649   5  4  2    2   58.7699  1.570622    0.0011  0.000028
   60.2193 1.536218   2  4  4    2   60.2242  1.536105    0.0049  0.000113
   60.9546 1.519426   5  7  0    2   60.9534  1.519454   -0.0012 -0.000028
   63.9213 1.455836   5  6  2    2   63.9203  1.455857   -0.0010 -0.000021

 rmse = 0.00002983819
 
     A =     9.6156(3)         B =    17.3513(7)          C =     6.9907(2)      
 Alpha =    90.             Beta =    90.             Gamma =    90.             
 
 Volume =   1166.37(5)