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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060086
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.043
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   24.6413 3.616104   2  2  0    2   24.6329  3.617315   -0.0084 -0.001212
   17.7493 5.005054   1  0  1    2   17.7413  5.007298   -0.0080 -0.002244
   12.2718 7.231862   1  1  0    2   12.2671  7.234631   -0.0047 -0.002768
   29.9657 2.983670   1  0  2    2   29.9628  2.983954   -0.0029 -0.000284
   26.6015 3.353488  -3  1  1    2   26.6000  3.353673   -0.0015 -0.000185
   39.3763 2.288787   2  4  0    2   39.3760  2.288805   -0.0003 -0.000017
   50.0457 1.822555  -2  0  4    2   50.0456  1.822558   -0.0001 -0.000002
   30.2928 2.952147  -3  0  2    2   30.2940  2.952029    0.0012  0.000119
   19.7619 4.498516   1  1  1    2   19.7633  4.498196    0.0014  0.000320
   17.3470 5.120500   0  2  0    2   17.3506  5.119435    0.0036  0.001065
   21.6991 4.100285  -1  2  1    2   21.7056  4.099071    0.0065  0.001214
   26.3572 3.384065   2  1  1    2   26.3669  3.382837    0.0097  0.001229

 rmse = 0.00003593501
 
     A =10.816(2)              B =10.239(1)               C =7.2907(4)           
 Alpha =90                  Beta =109.04(1)           Gamma =90                  
 
 Volume = 763.2(1)